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Construction of a multipurpose photochemical reactor with on-line spectrophotometric detection

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URI: http://hdl.handle.net/10498/20355

DOI: 10.1039/c5pp00407a

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2016-Construction of a multipurpose photochemical reactor with on-line spectrophotometric detection.pdf (1.369Mb)
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Author/s
Ditrói, Tamás; Kalmár, József; Pino-Chamorro, Jose Ángel; Erdei, Zsolt; Lente, Gábor; Fábián, István
Date
2016-02
Department
Ciencia de los Materiales e Ingeniería Metalúrgica y Química Inorgánica
Source
Photochem. Photobiol. Sci., 2016, 15, 589
Abstract
A versatile photoreactor was built for studying homogeneous and heterogeneous photochemical reactions using fiber-optic devices. The reactor was designed to allow simultaneous photochemical initiation and online spectrophotometric monitoring of the reaction using independently controlled excitation and detection lamps. The system consists of a CCD spectrophotometer, a thermostated sample holder, two light sources, and standard 1.00 × 1.00 cm (or possibly smaller) fluorescence cuvettes, all coupled with fiber optic cables. The device can be used as a photoreactor, a diode-array spectrophotometer and also as a spectrofluorimeter. The reactor can be used in flow-through operation modes. Performance tests of the instrument are reported here with a number of known photochemical systems.
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Attribution-NonCommercial-NoDerivatives 4.0 Internacional
This work is under a Creative Commons License Attribution-NonCommercial-NoDerivatives 4.0 Internacional

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