@misc{10498/24918, year = {2021}, month = {4}, url = {http://hdl.handle.net/10498/24918}, abstract = {An new method for the extraction of phenolic compounds from olive oil has been proposed before the chromatographic analysis by UPLC-PDA (Ultra-Performance Liquid Chromatography-PhotoDiode Array). Recoveries for 20 individual phenolic compounds were compared using three cartridges of solid-phase extraction including C-18, Diol, and DVB (DiVinylBenzene) based cartridges. Diol based cartridge produced the best retention efficiency. The optimized method uses a reduced amount of solvents and allows for the determination of most phenolics in oil samples in less than 10 min. A full discrimination among the most common olive oil varieties was achieved using the relative levels for specific phenolics in the sample. Therefore, based in this study, a fingerprint based on the relative levels for quercetin, luteolin, oleuropein and vanillic acid can be proposed to characterized varietal olive oils. In that way, a detailed composition about phenolic compounds of varietal olive oils would not be needed for discrimination purposes. (C) 2021 The Authors. Published by Elsevier B.V.}, publisher = {ELSEVIER}, keywords = {Discrimination}, keywords = {Olive oils}, keywords = {Olive varieties}, keywords = {Phenolic compounds}, keywords = {Solid-phase extraction (SPE)}, title = {Phenolic compounds in olive oil by solid phase extraction - Ultra performance liquid chromatography - Photodiode array detection for varietal characterization}, doi = {10.1016/j.arabjc.2021.103102}, author = {Deflaoui, L. and Setyaningsih, Widiastuti and Palma Lovillo, Miguel and Mekhoukhe, A. and Tamendjari, A.}, }