%0 Journal Article 
%A Sierra Padilla, Alfonso
%A Monari, A.
%A Palacios Santander, José María
%A García Guzmán, Juan José
%A Pigani, L.
%A Cubillana Aguilera, Laura
%T Electroanalysis of phenylalanine in food supplement by differential pulse voltammetry technique: Application of economical and handmade Sonogel-Carbon electrodes improved with a fast polarization step
%D 2025
%@ 0026-265X
%U http://hdl.handle.net/10498/36859
%X Sonogel-Carbon electrodes have been applied successfully in the determination of phenylalanine (Phe). These handmade economical sensor devices exhibit better electroanalytical performance than commercial electrodes, and by a fast surface polarization step the electrochemical signal was significantly increased. Improvements in the electrochemically active surface area and electrical conductivity were demonstrated. Excellent figures of merits were assessed, such as a sensitivity value of 68.19 ± 3.11 µA mM−1 cm−2 comparable to other previously reported devices and limit of detection of 31.92 ± 3.75 µM. Sonogel-Carbon electrodes exhibit worthy selectivity in the presence of other amino acids and electroactive species. Finally, satisfactory recovery values between 96 and 101 % were obtained when this material was applied in the determination of Phe in a food supplement sample. Sonogel-Carbon electrodes stand out compared to other reported sensor devices due to their simple, low-cost and eco-friendly manufacturing; their reusability; and their robust and selective electrochemical performance.
%K Electrochemical sensor
%K Sonogel-Carbon
%K Phenylalanine
%K Food supplement
%K Voltammetry
%~ Universidad de Cádiz