RT journal article T1 Systematic approach for high piezoelectric AlN deposition A1 Nieto Sierra, Lucía A1 Lloret Vieira, Fernando Manuel A1 Gallardo Bernal, Juan Jesús A1 García Núñez, Carlos A1 Pelayo García, Manuel A1 Alba Muñoz, Gonzalo A1 Gibson, Des A1 Araújo Gay, Daniel A2 Ciencia de los Materiales e Ingeniería Metalúrgica y Química Inorgánica A2 Física Aplicada A2 Química Física K1 Crystal structure; Microstructure; Piezoelectricity; Transmission electron microscopy; Vapor deposition K1 Crystal structure K1 Microstructure K1 Piezoelectricity K1 Transmission electron microscopy K1 Vapor deposition AB Aluminum nitride (AlN) is a wide band gap semiconductor with interesting piezoelectric properties for many applications, including micromechanical systems (MEMS), acoustic wave sensors or energy harvesting devices. The influence of DC reactive magnetron sputtering (DCRMS) deposition parameters on the structural, crystalline, and piezoelectric properties of AlN thin films are presented. The systematic approach of Design of Experiments (DoE) has been used to evaluate the role of magnetron power, nitrogen and argon flows on the deposition process and the film properties. Magnetron power and argon flow have resulted to be the parameters causing the most significant effects on the deposition rate. AlN films have been deposited with a high crystal quality, showing low values of FWHM (0.28) and c-axis orientation parallel oriented respect to the growth direction, as evidenced by X-ray diffraction (XRD) analysis and high-resolution transmission electron microscopy (HRTEM). These samples also showed a high piezoelectric coefficient (d33) of 5 pC/N for AlN thin films. This work highlights the importance of deposition parameters on the properties of the film and the important role that DoE play for its optimization with a minimum number of depositions. PB Elsevier SN 0925-8388 YR 2024 FD 2024 LK http://hdl.handle.net/10498/35812 UL http://hdl.handle.net/10498/35812 LA eng DS Repositorio Institucional de la Universidad de Cádiz RD 10-nov-2026